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Development of a low pressure syringe pump for detecting cannabinoids through liquid chromatography
(2022)
The following thesis covers the miniaturization and characterization of a pneumatic syringe pump, which is used for applications in low-pressure liquid chromatography. For this purpose, the components of the prototype are dealt with in the first section. These include the membrane pump and the cylinder for pressure and force generation, the syringe used for sample preparation and the construction of the test column. Furthermore, the pressure preparation on the cylinder, the friction losses of the syringe and then the behavior of the syringe in various application scenarios are considered. In the second section, the focus is on the different behaviors when using water and ethanol as a solvent. Tests in normal applications, as well as with air pockets or leaking seals, show the different behavior and the resulting deviations in the test pressure of the column. In addition, the maximum forces that can be applied to the syringe are worked out in several tests and the different maximum pressures, which depend on the solvent contained, are evaluated. These different maximum pressures, which are due to the different sealing behavior in connection with the surface tension of the liquid, will be discussed in conclusion. An outlook follows, up to which test pressures the system can be used and how these can be achieved.
Debugging errors in software applications can be a major challenge. It is not enough to know that a specific error exists, but the cause of it must be found in order to be able to fix it. Finding the source of an error can be time and cost intensive. The general approach is to analyse and debug the presumably erroneous part of the software. The analysis can be accompanied by instrumentation to gather additional information during the program execution. The analysis is made more difficult by the existence of different errors categories. Each category may need to be handled individually. Especially in embedded software applications, which commonly lack features like process or memory isolation, error detection and prevention can be even more challenging. This is the kind of problem this thesis tackles. This thesis tries to support developers during debugging and troubleshooting. The main focus is on errors related to memory management and concurrency. Specific features and properties of Arm Cortex-M processors are used to try to detect errors as well as their causes. For example, the memory protection unit is used to isolate the stack memories of different tasks running in a RTOS. The thesis tries to provide as much information as possible to the developer when reporting errors of any kind. The solution developed in this thesis also contains a custom memory allocator, which can be used to track down errors related to dynamic memory management. Furthermore, a Eclipse plugin has been developed which provides assertions for array accesses to detect and prevent out-of-bound accesses. The resulting solution has been implemented in commercial embedded software applications. This ensures that the developed solution is not only suitable for newly developed applications, but also for the integration into already existing products.
This is Intellectual Output 2 (IO2) of the project “Developing a culturally competent and compassionate LGBT+ curriculum in health and social care education“ IENE9. The aim of the project is to enable teacher/trainers of theory and practice to enhance their skills regarding LGBT+ issues and develop teaching tools to support the inclusion of LGBT+ issues within health and social care curricula. The newly culturally competent and compassionate LGBT+ curriculum will be delivered through a MOOC which is aimed at health and social care teachers/trainers, workers, professionals, and learners across Europe and worldwide. The IO2 of this project, Internet Mapping and Systematic documentation of educational policies and guidelines as well as legislation at European and national level for LGBT+ inclusive education, aims to create an easy to navigate resource with information about European and national legislation/guidance/policies. Visit www.iene-lgbt.com for more information.
Having autonomy in the workplace can have a positive impact on employees’ performance, which in turn can benefit the organization’s competitive advantages. While previous researches have primarily focused on the psychological effects of job autonomy on employee performance and has been limited to certain domains, the relationship between job autonomy and organizational design is an important area of study for organizations seeking to improve their competitiveness. This thesis proposes a conceptual model for designing an organization structure that promotes employee performance in manufacturing companies by removing obstacles towards obtaining job autonomy. The focus is on ambitious employees who seek growth and development opportunities within their organization. The model is based on a review of existing literature on job autonomy and organizational design. Exploratory qualitative research was conducted with selected ambitious employees from different industries by means of one-on-one semi-structured interviews. Overall, the proposed model has practical implications for manufacturing companies looking to motivate their employees, as well as for researchers seeking to advance their understanding of organizational design in our times.